化工社化工社 化学情報印刷レポート · 研究参考用
Benzenamine, 2-phenoxy- → 1-Isothiocyanato-2-phenoxybenzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzenamine, 2-phenoxy- | HCID 75899 | — |
| 反応物 | Thiocarbonyl diimidazole | HCID 11412697 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 1-Isothiocyanato-2-phenoxybenzene | HCID 22040439 | — |
反応手順
1.96 g (0.011 mol) of thiocarbonyl diimidazole were added to a solution of 1.85 g (0.01 mol) of 2-phenoxyaniline in 50 ml of THF and the mixture was stirred at room temperature for 4 hours, giving, after removal of the solvent by distillation, the compound as a brown amorphous product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07179829B2 |
| 出典データセット | uspto-grants-2007_02 |
| ORD ID | ord-853bee71781a42c6a85dc3d3c78adb8d |
| 出典メモ | uspto-grants-2007_02 |