化工社化工社 化学情報印刷レポート · 研究参考用
Diisopropylethylamine → N-(3-Amino-4-thienyl)-N'-(2,6-dimethylphenyl)thiourea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diisopropylethylamine | HCID 81531 | — |
| 反応物 | 2,6-Xylyl isothiocyanate | HCID 87976 | — |
| 反応物 | Thiophene-3,4-diamine dihydrobromide | HCID 21989329 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | N-(3-Amino-4-thienyl)-N'-(2,6-dimethylphenyl)thiourea | HCID 86037743 | — |
反応手順
was obtained in a similar manner to the method specified in Example 6a) by reacting a mixture prepared from 0.74 g of N-ethyl-N,N-diisopropylamine in 40 ml of THF, 0.8 g of 3,4-diaminothiophene dihydrobromide and 0.47 g of 2,6-dimethylphenyl isothiocyanate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07179830B2 |
| 出典データセット | uspto-grants-2007_02 |
| ORD ID | ord-55ab235eef0b408d86fc24fc8d6b7ba4 |
| 出典メモ | uspto-grants-2007_02 |