化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 5-Bromofuran-2-carbonyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 5-Bromo-2-furanecarboxylic acid | HCID 68511 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 5-Bromofuran-2-carbonyl chloride | HCID 2757011 | — |
反応手順
21.0 g of 5-bromo-2-furancarboxylic acid were suspended in 650 ml of toluene and 40 ml of thionyl chloride and the suspension was heated to reflux for 2 hours. The reaction solution was thereafter concentrated, whereby 5-bromo-2-furancarboxylic acid chloride was obtained as the residue.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04764522 |
| 出典データセット | uspto-grants-1988_08 |
| ORD ID | ord-374bfbb4f33346df9af44276ccb38c16 |
| 出典メモ | uspto-grants-1988_08 |