化工社化工社 化学情報印刷レポート · 研究参考用
2-Hydroxy-4-morpholin-4-yl-benzaldehyde → 1-(2-Hydroxy-4-morpholin-4-yl-phenyl)-propan-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Hydroxy-4-morpholin-4-yl-benzaldehyde | HCID 9815659 | — |
| 反応物 | HCID 178418443 | HCID 178418443 | — |
| 生成物 | 1-(2-Hydroxy-4-morpholin-4-yl-phenyl)-propan-1-one | HCID 9964689 | — |
反応手順
Following the procedure for preparing Example 34, 4-(4-morpholinyl)-salicylaldehyde (1.0 g, 5 mmol) and ethylmagnesium bromide (1.0 M solution in tetrahydrofuran, 11 mL, 11 mmol) were converted to the product (208 mg, 18%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07179912B2 |
| 出典データセット | uspto-grants-2007_02 |
| ORD ID | ord-c2724d3583464f398d8246c235623b68 |
| 出典メモ | uspto-grants-2007_02 |