化工社化工社 化学情報印刷レポート · 研究参考用
3-Ethoxy-4-nitrobenzoic acid → 4-Amino-3-ethoxybenzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Ethoxy-4-nitrobenzoic acid | HCID 22397509 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 生成物 | 4-Amino-3-ethoxybenzoic acid | HCID 22397448 | 92.1% |
反応手順
3-Ethoxy-4-nitrobenzoic acid (0.31 g) was treated with 5% palladium on charcoal under an atmosphere of hydrogen (1 bar) for 3 hours. The reaction mixture was filtered and the filtrate was evaporated to leave the product as a beige solid (0.245 g; MS: ES− (M−H) 180).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07179922B2 |
| 出典データセット | uspto-grants-2007_02 |
| ORD ID | ord-c7e399d3d7ad4676891392da5b623124 |
| 出典メモ | uspto-grants-2007_02 |