化工社化工社 化学情報印刷レポート · 研究参考用
Oxalic acid dihydrate → N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide oxalate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxalic acid dihydrate | HCID 61373 | — |
| 反応物 | N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide | HCID 67930011 | — |
| 生成物 | N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide oxalate | HCID 67930072 | 80% |
反応手順
The procedure of Example 7 was repeated using 917 mg (2.36 mmol.) of N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide and 298 mg (2.36 mmol.) of oxalic acid dihydrate, to obtain 901 mg (yield: 80%) of the subject compound as a whilte crystalline product upon recrystallization from 8 ml of ethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04764617 |
| 出典データセット | uspto-grants-1988_08 |
| ORD ID | ord-d189332df8ad49bc8a8152b0d3067aa0 |
| 出典メモ | uspto-grants-1988_08 |