反応式
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH2:18]([S-:20])[CH3:19].[Na+]>C(S)C>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]([S:20][CH2:18][CH3:19])=[NH:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1参加物
4
実験手順
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and sodium ethanethiolate in ethanethiol there is obtained ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate and therefrom with hydrochloric acid in alcohol there is obtained the hydrochloride, m.p. 220° C. (with decomposition);
出典と根拠
- ORDレコード
- ord-9b579c6ea71c44829cf397c559a47b98
- 出典データセット
- uspto-grants-1988_08
- 特許番号
- US04766115
関連ノート
読み込み中…