関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethyl methanesulfonylacetate | HCID 78201 | — |
| 反応物 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 生成物 | Ethyl 3-dimethylamino-2-methylsulphonylacrylate | HCID 57126670 | — |
反応手順
6.65 g (40 mmol) of ethyl methanesulphonylacetate and 5.72 g (48 mmol) of N,N-dimethylformamide dimethyl acetal are admixed and heated at 85° C. overnight. The solution is concentrated using a rotary evaporator, and the solid is comminuted with cyclohexane and filtered off with suction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06743798B1 |
|---|
| 出典データセット | uspto-grants-2004_06 |
|---|
| ORD ID | ord-d5b98d3c965f4e9796d425aac5851886 |
|---|
| 出典メモ | uspto-grants-2004_06 |
|---|
