化工社化工社 化学情報印刷レポート · 研究参考用
2-Allylphenol → Benzoxazines
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Allylphenol | HCID 15624 | — |
| 反応物 | Aminopropyltrimethoxysilane | HCID 83756 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Benzoxazines | HCID 17845026 | 94% |
反応手順
This compound was prepared according to the method described in the previous examples using 3-aminopropyltrimethoxysilane (17.9 g, 100 mmole), paraformaldehade (6.3 g, 210 mmole), 2-allyl-phenol (13.4 g, 0.1 mmole), and toluene (200 ml). The final product was obtained as a slightly yellow, mobile liquid. The yield was 94% of theory.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06743852B2 |
| 出典データセット | uspto-grants-2004_06 |
| ORD ID | ord-6358ad625d7f4fa781932705f29eec87 |
| 出典メモ | uspto-grants-2004_06 |