Ethylenediamine → Benzoxazines

HRID 351953

反応式

HRID 351953 の反応式
[CH2:1]([NH2:4])[CH2:2]N.C([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[OH:14])C=C>C1(C)C=CC=CC=1>[O:14]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[CH:2]=[CH:1][NH:4]1

参加物

4

反応物 2

HCID 3301EthylenediamineHCID 156242-Allylphenol

生成物 1

HCID 17845026Benzoxazines収率 92%

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

This compound was prepared according to the method described in the previous examples from ethylene diamine (6.0 g, 100 mmole), paraformaldehade (12.6 g, 420 mmole), 2-allyl-phenol (26.8 g, 200 mmole), and toluene (200 ml). The final product was obtained as a viscous liquid. The yield was 92% of theory.

後処理

  1. customThis compound was prepared

出典と根拠

ORDレコード
ord-b73088da909247a5be0fc91e9eb148c5
出典データセット
uspto-grants-2004_06
特許番号
US06743852B2

関連ノート

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