化工社化工社 化学情報印刷レポート · 研究参考用
Formaldehyde → Benzoxazines
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formaldehyde | HCID 712 | — |
| 反応物 | (3-Aminopropyl)triethoxysilane | HCID 13521 | — |
| 反応物 | 1-(4-hydroxyphenyl)-1H-pyrrole-2,5-dione | HCID 81734 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Benzoxazines | HCID 17845026 | 37% |
反応手順
This compound was prepared according to the method used for the previous examples by combining 4-maleimidophenol (18.9 g, 100 mmol), 3-aminopropyltriethoxysilane (22.1 g, 100 mmol), paraformaldehyde (6.3 g, 210 mmol), and toluene (150 mL). The final product was a highly viscous red liquid. The yield was 37%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06743852B2 |
| 出典データセット | uspto-grants-2004_06 |
| ORD ID | ord-ccafa9c809e64946a0be199b17c9234d |
| 出典メモ | uspto-grants-2004_06 |