化工社化工社 化学情報印刷レポート · 研究参考用
Hexane → cis-Stilbene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexane | HCID 8058 | — |
| 反応物 | Diphenylacetylene | HCID 10390 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | cis-Stilbene | HCID 5356785 | — |
反応手順
In the foregoing epititanations of diphenylacetylene conducted in THF or hexane, parallel epititanations were conducted in the same manner but the hydrolytic workup in each case was performed with 3N DCl in D2O. In these experiments the cis-stilbene isolated was >98% dideuteriated at the vinylic carbon atoms (12).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06743872B1 |
| 出典データセット | uspto-grants-2004_06 |
| ORD ID | ord-9507fa7fcc184888bfcbd3570c598bd7 |
| 出典メモ | uspto-grants-2004_06 |