関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Thioglycolic Acid | HCID 1133 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Benzoic acid, 2,4-dichloro-, ethyl ester | HCID 42026 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Ethyl 4-carboxymethylsulfenyl-2-chlorobenzoate | HCID 12993801 | — |
反応手順
A mixture containing ethyl 2,4-dichlorobenzoate (10.0 g), potassium carbonate (9.44 g), dimethylformamide (50 ml), and mercaptoacetic acid (3.8 ml) was allowed to react with heat at 80° C. for 4 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06756343B1 |
|---|
| 出典データセット | uspto-grants-2004_06 |
|---|
| ORD ID | ord-c042bd80104540ff8b5020c5211258d2 |
|---|
| 出典メモ | uspto-grants-2004_06 |
|---|
