化工社化工社 化学情報印刷レポート · 研究参考用
Dichlorodiphenylsilane → Diphenyl bis(3,5,6-trichloro-2-pyridyloxy)silane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dichlorodiphenylsilane | HCID 6627 | — |
| 反応物 | Methyl 3,5,6-trichloro-2-pyridyl carbonate | HCID 20218094 | — |
| 触媒 | Tetrabutylammonium Chloride | HCID 70681 | — |
| 生成物 | Diphenyl bis(3,5,6-trichloro-2-pyridyloxy)silane | HCID 20508437 | — |
反応手順
In the manner described in Examples 1-7, diphenyldichlorosilane was reacted with about two moles of methyl 3,5,6-trichloro-2-pyridyl carbonate in the presence of tetrabutylammonium chloride to produce a good yield of diphenyl bis(3,5,6-trichloro-2-pyridyloxy)silane, a crystalline solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04375549 |
| 出典データセット | uspto-grants-1983_03 |
| ORD ID | ord-33bc60857ac645f1a3e3a467526a3167 |
| 出典メモ | uspto-grants-1983_03 |