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llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
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Ammonia → Stearic Acid

HRID 354620
ノート
印刷プレビュー

反応式

HRID 354620 の反応式
[O-2].[Zn+2:2].N.C(=O)=[O:5].[C:7]([OH:26])(=[O:25])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>O>[O-2:5].[Zn+2:2].[C:7]([OH:26])(=[O:25])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24].[C:7]([O-:26])(=[O:25])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24].[Zn+2:2].[C:7]([O-:26])(=[O:25])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

8

反応物 4

HCID 222Ammonia2 回HCID 280Carbon DioxideHCID 5281Stearic AcidHCID 3007857Zinc Oxide

生成物 3

HCID 5281Stearic AcidHCID 11178Zinc StearateHCID 3007857Zinc Oxide

試薬・触媒・溶媒

1
HCID 962Water溶媒2 回

反応条件

温度
80 °C

実験手順

130 kg of zinc oxide is dispersed in a rotor-stator shear machine with 16 liters of 25% aqueous ammonia in 480 liters of cold water with simultaneous introduction of gaseous carbon dioxide. Simultaneously, 900 kg of molten stearic acid is emulsified at 80° C. in 180 liters of water and to the emulsion there is added 36 liters of 25% aqueous ammonia. Both dispersions are fed at 80° C. through correspondingly adjusted dosing pumps to a rotor-stator shear machine likewise heated to 80° C., so that stoichiometric amounts are reacted per unit of time. From the 130 kg of zinc oxide and 900 kg of stearic acid (saponification number=204) there is formed 1000 kg of zinc stearate. The pasty zinc stearate drawn off from the rotor-stator shear machine has a water content of about 45%. It is fed directly to a flowing air dryer in which it is dried to a water content of 0.2%. The end product is a finely granular, extremely pure, electrolyte-free zinc stearate.

後処理

  1. customare fed at 80° C. through correspondingly adjusted dosing pumps to a rotor-stator shear machine
  2. customare reacted per unit of time

出典と根拠

ORDレコード
ord-548ecfa34cb84a7d8c942fa974dd25bb
出典データセット
uspto-grants-1983_03
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04376079

反応ノート

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