化工社化工社 化学情報印刷レポート · 研究参考用
Anthranilic Acid → 2-Amino-4-methoxybenzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Anthranilic Acid | HCID 227 | — |
| 反応物 | Ammonium Hydroxide | HCID 14923 | — |
| 反応物 | 4-Methoxy-2-nitrobenzoic acid | HCID 288657 | — |
| 生成物 | 2-Amino-4-methoxybenzoic acid | HCID 351010 | — |
反応手順
A solution of 4-methoxy-2-nitrobenzoic acid (19.3 g., 97.9 mmole) of 200 ml. 1 N NH4OH was reduced overnight in presence of 5% Pd/BaCO3. The reaction mixture was filtered and acidified with acetic acid to yield 15.8 g. (96%) of the anthranilic acid, M.P. 186°-188° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04377581 |
| 出典データセット | uspto-grants-1983_03 |
| ORD ID | ord-50a7b5b4e30d473090bcc1d5854a60ba |
| 出典メモ | uspto-grants-1983_03 |