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Hydrogen Bromide → 2-Benzyl benzylbromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | 2-Benzylbenzyl alcohol | HCID 74109 | — |
| 生成物 | 2-Benzyl benzylbromide | HCID 12422098 | 98% |
反応手順
2-Benzylbenzyl alcohol (commercial) (1 g) was suspended in 48% aqueous hydrobromic acid (10 ml) and stirred vigorously for 20 hours. The resultant suspended solid was extracted twice with hexane and the extracts dried (MgSO4) and evaporated to give 2-benzyl benzylbromide as yellow solid (1.3 g, 98%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05834468 |
| 出典データセット | uspto-grants-1998_11 |
| ORD ID | ord-93f2795254ed44abb88915047391a63e |
| 出典メモ | uspto-grants-1998_11 |