2,8-Diacetylamino-1-tetralone → 2-Acetylamino-8-amino-5-methyl-1-tetralone

HRID 355963ノート

反応式

HRID 355963 の反応式
[C:1]([NH:4][CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([NH:16]C(=O)C)[CH:9]=[CH:10][C:11]=2[CH3:15])[C:6]1=[O:20])(=[O:3])[CH3:2].C(NC1CCC2C(=C(NC(=O)C)C=CC=2)C1=O)(=O)C>>[C:1]([NH:4][CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([NH2:16])[CH:9]=[CH:10][C:11]=2[CH3:15])[C:6]1=[O:20])(=[O:3])[CH3:2]

参加物

3

反応物 2

HCID 120472982,8-Diacetylamino-1-tetraloneHCID 867509612,8-Diacetylamino-5-methyl-1-tetralone

生成物 1

HCID 224494492-Acetylamino-8-amino-5-methyl-1-tetralone

実験手順

The reaction was carried out in the same manner as in Example 1-(4), except that 400 mg of the compound prepared in (7) above was used instead of 2,8-diacetylamino-1-tetralone of Example 1-(4), and post-treated to produce 265 mg of the title compound.

後処理

  1. additionpost-treated

出典と根拠

ORDレコード
ord-5c36ab79f2e04e778313519007891dd5
出典データセット
uspto-grants-1998_11
特許番号
US05834476

反応ノート

読み込み中…