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1-Acetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one → 1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Acetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one | HCID 10353298 | — |
| 反応物 | N-(8-Oxo-5,6,7,8-tetrahydronaphthalen-1-YL)acetamide | HCID 12119265 | — |
| 生成物 | 1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one | HCID 22449453 | — |
反応手順
The reaction was carried out in the same manner as in Example 1-(2), except that 270 mg of the compound prepared in (2) above was used instead of 8-acetylamino-1-tetralone of Example 1-(2). The reaction mixture obtained by the post-treatment was further reacted in the same manner as in Example 1-(3) and post-treated to produce 126 mg of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05834476 |
| 出典データセット | uspto-grants-1998_11 |
| ORD ID | ord-a6c9eea160d542618b7334d21eca165d |
| 出典メモ | uspto-grants-1998_11 |