化工社化工社 化学情報印刷レポート · 研究参考用
4-Mercaptophenol → 4-[(4-Hydroxyphenyl)disulfanyl]phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Mercaptophenol | HCID 240147 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | 4-[(4-Hydroxyphenyl)disulfanyl]phenol | HCID 280665 | — |
反応手順
p-Hydroxybenzenethiol (25 g) was dissolved in DMSO (155 ml) and the solution was stirred for 4 hours and poured into ice water (1 L). The precipitated crystals were dried under reduced pressure to give bis(p-hydroxyphenyl)disulfide quantitatively.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05840716 |
| 出典データセット | uspto-grants-1998_11 |
| ORD ID | ord-7085146c16bc4d318e7e2210028e4e8b |
| 出典メモ | uspto-grants-1998_11 |