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Methanol → 1-Methyl-3,5-diphenylpyrazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 1H-Pyrazole, 3,5-diphenyl- | HCID 70840 | — |
| 生成物 | 1-Methyl-3,5-diphenylpyrazole | HCID 140517 | 91% |
反応手順
A total of 181.5 g (0.825 mol) of 3,5-diphenylpyrazole and 791 g (24.7 mol) of methanol was used. A total of 175.8 g (91%) of 1-methyl- 3,5-diphenylpyrazole was obtained. The holdup of the bubble column was not taken into account.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05840913 |
| 出典データセット | uspto-grants-1998_11 |
| ORD ID | ord-78cf8971f53a467a8ff0bc6babcc370a |
| 出典メモ | uspto-grants-1998_11 |