化工社化工社 化学情報印刷レポート · 研究参考用
Dimethylamine → 2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | Chlorosulfonic acid | HCID 24638 | — |
| 反応物 | O-ethylhydroxylamine hydrochloride | HCID 76850 | — |
| 反応物 | HCID 178458832 | HCID 178458832 | — |
| 生成物 | 2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one | HCID 135973980 | — |
反応手順
2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one (5) was prepared from 3-hydroxy-5-(2,6-dimethylphenyl)-2-propionylcyclohex-2-en-1-one, chlorosulfonic acid, dimethylamine, and ethoxyamine hydrochloride following essentially the same procedure as that described in Example 5.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04767879 |
| 出典データセット | uspto-grants-1988_08 |
| ORD ID | ord-5cb6474f52844c2bba022377de34628a |
| 出典メモ | uspto-grants-1988_08 |