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1-Undecanol → Undecyl propylcarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Undecanol | HCID 8184 | — |
| 反応物 | Propyl isocyanate | HCID 61033 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | Undecyl propylcarbamate | HCID 20450444 | 89% |
反応手順
For example, 8.6 g (50 mmol) of 1-undecanol, 5 ml (1.07 eq.) n-propyl isocyanate and 50 ml diethyl ether were heated in a stainless steel bomb at 65° for 72 hours. Solvent and excess isocyanate were removed on a rotary evaporator and the residue was crystallized from hexane to give 11.5 g (89%) of 1-undecyl propylcarbamate, mp 45°-45.5°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04464390 |
| 出典データセット | uspto-grants-1984_08 |
| ORD ID | ord-7680ec264add46dfacb03dcd0912bcbd |
| 出典メモ | uspto-grants-1984_08 |