Dodecanoyl chloride → 2-[(2-Dodecanoyloxyacetyl)-(2-dodecanoyloxyethyl)amino]ethyl dodecanoate

HRID 358101

反応式

HRID 358101 の反応式
[C:1](Cl)(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[OH:15][CH2:16][CH2:17][N:18]([CH2:23][CH2:24][OH:25])[C:19](=[O:22])[CH2:20][OH:21]>>[C:1]([O:15][CH2:16][CH2:17][N:18]([CH2:23][CH2:24][O:25][C:1](=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[C:19](=[O:22])[CH2:20][O:21][C:1](=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

参加物

3

反応物 2

HCID 8166Dodecanoyl chlorideHCID 87097N,N-Bis(2-hydroxyethyl)glycolamide

生成物 1

HCID 3267942-[(2-Dodecanoyloxyacetyl)-(2-dodecanoyloxyethyl)amino]ethyl dodecanoate

実験手順

This compound was prepared from 131 g (0.6 mole) of lauroyl chloride and 32.6 g (0.2 mole) of N,N-bis(hydroxyethyl) hydroxyacetamide by the procedure of Example 1. Its structure was established by infrared and nuclear magnetic resonance spectroscopy. It was a low-melting solid and had n30D 1.4597 and m.p. 29.6° C.

出典と根拠

ORDレコード
ord-441e4df9c7b5444a945a842f5322543b
出典データセット
uspto-grants-1984_08
特許番号
US04464392

関連ノート

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