Isopropanol → Isopropyl Trichloroacrylate
反応式
[CH:1]([OH:4])([CH3:3])[CH3:2].[Cl:5][C:6](=[C:10]([Cl:12])[Cl:11])[C:7](Cl)=[O:8]>C(Cl)Cl>[Cl:11][C:10]([Cl:12])=[C:6]([Cl:5])[C:7]([O:4][CH:1]([CH3:3])[CH3:2])=[O:8]参加物
4
実験手順
A solution of 6.5 gms (0.108 moles) isopropyl alcohol, 20 gms (0.013 moles) trichloro acryloyl chloride and 100 ml methylene chloride was stirred for 72 hours. The solvent was stripped and the product was used in subsequent reactions without further purification.
後処理
- customthe product was used in subsequent reactions without further purification
出典と根拠
- ORDレコード
- ord-4cc9112742054be59544a64647003c56
- 出典データセット
- uspto-grants-1984_08
- 特許番号
- US04465690
反応ノート
読み込み中…