Butyl Benzoate → Titanium trichloride butyl benzoate
反応式
[Cl-:1].[Cl-].[Cl-].[Ti+3:4].[C:5]([O:13][CH2:14][CH2:15][CH2:16][CH3:17])(=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>C1(C)C=CC=CC=1>[Cl-:1].[Cl-:1].[Cl-:1].[Ti+3:4].[C:5]([O:13][CH2:14][CH2:15][CH2:16][CH3:17])(=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1参加物
4
実験手順
The mixture which was homogenised consisted of 119 g of titanium trichloride, 26 cm3 of butyl benzoate, 390 cm3 of toluene and 3 g of polystyrene ("Lustrex" HF 66). After operating the homogeniser at maximum power for 2.75 minutes, the contents of the flask had formed an immobile gel-like product and the temperature had risen to above 50° C. Homogenisation was terminated and 500 cm3 of toluene were added to assist in the transfer of the dispersed solid to a storage vessel.