Methyl isothiocyanate → HCID 178486097、化合物
反応式
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:9]=[CH:10][NH:11][CH:12]=2)=[CH:4][CH:3]=1.[CH3:13][N:14]=[C:15]=[S:16]>C(O)C>[CH3:13][NH:14][C:15]([NH:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[N:9]=[CH:10][NH:11][CH:12]=2)=[CH:6][CH:7]=1)=[S:16]参加物
4
実験手順
A solution of 2.3 gm of 4-(4-aminophenyl)-1-H-imidazole and 1.15 gm of methyl isothiocyanate in 30 ml of ethanol was refluxed for thirty minutes and evaporated to dryness. The oily base so obtained was purified by conversion into the corresponding hydrochloride salt by bubbling gaseous hydrochloric acid in isopropanol. The desired thiourea was obtained as a white solid.
後処理
- customevaporated to dryness
- customThe oily base so obtained
- customwas purified by conversion into the corresponding hydrochloride salt
- customby bubbling gaseous hydrochloric acid in isopropanol
出典と根拠
- ORDレコード
- ord-3b6a72acc242468fa129b70ab27e32a6
- 出典データセット
- uspto-grants-1984_08
- 特許番号
- US04465841
反応ノート
読み込み中…