化工社化工社 化学情報印刷レポート · 研究参考用
4-Chlorobenzenesulfonyl chloride → 7-(4-Chlorobenzenesulphonamido)heptanoic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| 反応物 | 7-Aminoheptanoic acid | HCID 13580 | — |
| 溶媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | 7-(4-Chlorobenzenesulphonamido)heptanoic Acid | HCID 20066980 | — |
反応手順
A solution of 7-aminoheptanoic acid in 10% sodium hydroxide solution was treated with 4-chlorobenzenesulphonyl chloride in the manner of Example 1 to give the title compound which, after recrystallisation from aqueous ethanol, had a melting point of 128°-129° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04997847 |
| 出典データセット | uspto-grants-1991_03 |
| ORD ID | ord-c812be37b9ed44eb8f0793de2ca21202 |
| 出典メモ | uspto-grants-1991_03 |