Ammonia → Benzenesulfinamide

HRID 358746

反応式

HRID 358746 の反応式
[C:1]1([S:7](Cl)=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH3:10]>CCOCC>[C:1]1([S:7]([NH2:10])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

参加物

4

反応物 2

HCID 222AmmoniaHCID 4190003Benzenesulfinyl chloride

生成物 1

HCID 11286519Benzenesulfinamide収率 17%

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

Benzenesulphinamide was prepared by reacting benzenesulphinyl chloride with ammonia in ether initially at -78° C. and finally at ambient temperature and was isolated in 17% yield as a solid, m.p. 112°-115° C.

後処理

  1. custominitially at -78° C.
  2. customfinally at ambient temperature and was isolated in 17% yield as a solid, m.p. 112°-115° C.

出典と根拠

ORDレコード
ord-61f89b91a1154459a9933bf9d6056d4e
出典データセット
uspto-grants-1991_03
特許番号
US04997844

関連ノート

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