化工社化工社 化学情報印刷レポート · 研究参考用
3-Methyl-2-buten-1-OL → Ethyl 3,3-dimethylpent-4-enoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Methyl-2-buten-1-OL | HCID 11173 | — |
| 反応物 | Ethyl ortho-acetate | HCID 86598186 | — |
| 触媒 | Phosphoric Acid | HCID 1004 | — |
| 生成物 | Ethyl 3,3-dimethylpent-4-enoate | HCID 82262 | 79% |
反応手順
A mixture of 4.3 g of 3-methyl-2-buten-1-ol, 16.2 g of ethyl orthoacetate and 3 drops of phosphoric acid was reacted as described in Example V A to give 6.15 g (79% yield) of ethyl 3,3-dimethyl-4-pentenoate, b.p. 87°-88°/58 mm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04999451 |
| 出典データセット | uspto-grants-1991_03 |
| ORD ID | ord-3e7cb3b1ca404cda836c93bd7abb5b97 |
| 出典メモ | uspto-grants-1991_03 |