化工社化工社 化学情報印刷レポート · 研究参考用
4-Octylaniline → N-(p-octylphenyl)-2,4,6-triphenylpyridinium triflate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Octylaniline | HCID 85346 | — |
| 反応物 | AG-G-77560 | HCID 2778031 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-(p-octylphenyl)-2,4,6-triphenylpyridinium triflate | HCID 20064818 | — |
反応手順
A 4.58-g portion (0.01 mole) of 2,4,6-triphenylpyrylium triflate is added to 200 ml of ethanol. To this solution, 2.05 g (0.01 mole) of p-n-octylaniline is added. The mixture is refluxed for about 20 hours. Upon removing the ethanol by rotating evaporation, an orange oil remains. To remove the last of the ethanol the oil is placed under high vacuum.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05000873 |
| 出典データセット | uspto-grants-1991_03 |
| ORD ID | ord-7852d11320734bafb0ba94ae0caa2fb1 |
| 出典メモ | uspto-grants-1991_03 |