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4-Dodecylaniline → HCID 20064821、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Dodecylaniline | HCID 7701 | — |
| 反応物 | AG-G-77560 | HCID 2778031 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 20064821 | HCID 20064821 | — |
反応手順
A 2.3-g portion (0.005 mole) of 2,4,6-triphenylpyrylium triflate is placed in a 500-ml round-bottom flask. To this, 200 ml of ethanol is added and then 1.3 g (0.005 mole) of p-dodecylaniline is added. The mixture is refluxed for about 20 hours. The ethanol is removed by evaporation to give a yellow waxy substance. This material is washed with ether which causes some yellow crystals to precipitate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05000873 |
| 出典データセット | uspto-grants-1991_03 |
| ORD ID | ord-7f3fcc1c6d9047fca8c49414a0df1a8c |
| 出典メモ | uspto-grants-1991_03 |