1-Bromopropane → HCID 18963354、化合物

反応式

[C:1]([C:4]1[CH2:9][CH2:8][CH2:7][NH:6][CH:5]=1)(=[O:3])[CH3:2].Br[CH2:11][CH2:12][CH3:13].CC(N1CCCC(C(C)=O)=C1)C>>[CH2:11]([N:6]1[CH2:7][CH2:8][CH2:9][C:4]([C:1]([CH3:2])=[O:3])=[CH:5]1)[CH2:12][CH3:13]

参加物

反応物 3

HCID 78401-Bromopropane

HCID 32845951-(1,4,5,6-Tetrahydropyridin-3-yl)ethanone

HCID 18963350HCID 18963350、化合物

生成物 1

HCID 18963354HCID 18963354、化合物

実験手順

Methyl 1-propyl-1,4,5,6-tetrahydro-3-pyridyl ketone was prepared from 3-acetyl-1,4,5,6-tetrahydropyridine and 1-bromopropane according to the procedure of Part (b) of Example 1. The product distilled as a pale yellow (b.pt98-100°C./0.5 mm Hg).