Methyl 1-(2-phenylethyl)-1,4,5,6-tetrahydro-3-pyridyl ketone → Propyl 1-propyl-1,4,5,6-tetrahydro-3-pyridyl ketone
反応式
[Br-].[CH2:2]([N+:5]1[CH:10]=[CH:9][CH:8]=[C:7]([C:11](=[O:15])[CH2:12][CH2:13][CH3:14])[CH:6]=1)[CH:3]=[CH2:4].C1(CCN2CCCC(C(C)=O)=C2)C=CC=CC=1>>[CH2:2]([N:5]1[CH2:10][CH2:9][CH2:8][C:7]([C:11]([CH2:12][CH2:13][CH3:14])=[O:15])=[CH:6]1)[CH2:3][CH3:4]参加物
3
実験手順
1-(2-Propenyl)-3-butyryl pyridinium bromide was hydrogenated according to the procedure described in Part (b) of Example 6 to give propyl 1-propyl-1,4,5,6-tetrahydro-3-pyridyl ketone. The product was distilled as a pale yellow oil (b.pt 150-153°C./0.3 mm Hg)
出典と根拠
- ORDレコード
- ord-e3f19aebb1074bc7ac4c7ff0c47d1fae
- 出典データセット
- uspto-grants-1991_03
- 特許番号
- US05000946
反応ノート
読み込み中…