関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Acetone Cyanohydrin | HCID 6406 | — |
| 反応物 | 4-Amino-1-butanol | HCID 25868 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 2-((4-Hydroxybutyl)amino)-2-methylpropanenitrile | HCID 15511961 | — |
反応手順
220 μl of acetone cyanohydrin and 200 μl of 4-amino 1-butanol were mixed together with stirring for 16 hours at 20° C. and then was diluted with 2 ml of methylene chloride, dried, filtered and the filtrate was concentrated under reduced pressure to obtain the propanonitrile which was used as is for the following stage.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05411981 |
|---|
| 出典データセット | uspto-grants-1995_05 |
|---|
| ORD ID | ord-af507ea0ea16417b8b65e6f6abd9ae52 |
|---|
| 出典メモ | uspto-grants-1995_05 |
|---|
