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Anthranilamide → N-[(2-carbamoylphenyl)carbamothioyl]-3-methylbenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Anthranilamide | HCID 6942 | — |
| 反応物 | 3-Methylbenzoyl isothiocyanate | HCID 141397 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | N-[(2-carbamoylphenyl)carbamothioyl]-3-methylbenzamide | HCID 667545 | 89.3% |
反応手順
To a stirred mixture of 7.2 g of 2-aminobenzamide and 200 ml of ether was added dropwise, a solution of 10 g of 3-methylbenzoyl isothiocyanate over 10 minutes. After 48 hours, the solid was collected, giving 14.8 g of the desired product as grey crystals, mp 194°-196° (dec.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05001157 |
| 出典データセット | uspto-grants-1991_03 |
| ORD ID | ord-0d79b3cbfe21472dbe9de27f6fa957f8 |
| 出典メモ | uspto-grants-1991_03 |