関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Imidazole | HCID 795 | — |
| 反応物 | 1-(Bromomethyl)-3-[[3-(hexadecyloxy)-2-methoxypropoxy]methyl]benzene | HCID 19939557 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 1-[[3-[[3-(Hexadecyloxy)-2-methoxypropoxy]methyl]phenyl]methyl]-1H-imidazol | HCID 19939546 | 86.3% |
反応手順
a mixture of 2.4 g of 1-(bromomethyl)-3-[[3-(hexadecyloxy)-2-methoxypropoxy]methyl]benzene, 2.54 g of imidazole and 30 ml of toluene was heated at 80° C. under argon in a pressure bottle for 4 hours and then evaporated. The residue was purified by chromatography, giving 2.02 g of the desired product as a colorless oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05411983 |
|---|
| 出典データセット | uspto-grants-1995_05 |
|---|
| ORD ID | ord-786f211439ef46fe9014490b5ebd34f7 |
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| 出典メモ | uspto-grants-1995_05 |
|---|
