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Allylamine → 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Allylamine | HCID 7853 | — |
| 反応物 | 1,1'-Dimethyl 2,2'-(1,2-diazenediyl)bis(2-methylpropanoate) | HCID 75763 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide] | HCID 15724735 | — |
反応手順
Dimethyl 2,2'-azobis(2-methylpropionate) in an amount of 41.9 g, 48 ml of methanol, and 43 g of a 28% CH3ONa methanol solution were mixed and stirred for dissolution, followed by dropwise addition of 25 g of allylamine to react at 19° to 21° C. for 20 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05001228 |
| 出典データセット | uspto-grants-1991_03 |
| ORD ID | ord-cbc849f2079f4b2e89bfcd0e603da8a8 |
| 出典メモ | uspto-grants-1991_03 |