N,N-Diethylethylenediamine → 4-([2-(N,N-diethylamino)ethyl]aminocarbonyl)benzoic acid
反応式
C(O[C:9]([C:11]1[CH:19]=[CH:18][C:14]([C:15]([OH:17])=[O:16])=[CH:13][CH:12]=1)=[O:10])C1C=CC=CC=1.[CH2:20]([N:22]([CH2:26][CH3:27])[CH2:23][CH2:24][NH2:25])[CH3:21]>>[CH2:20]([N:22]([CH2:23][CH2:24][NH:25][C:9]([C:11]1[CH:12]=[CH:13][C:14]([C:15]([OH:17])=[O:16])=[CH:18][CH:19]=1)=[O:10])[CH2:26][CH3:27])[CH3:21]参加物
3
実験手順
4-([2-(N,N-diethylamino)ethyl]aminocarbonyl)benzoic acid was prepared from 4-benzyloxycarbonylbenzoic acid by reaction with N,N-diethylethylene diamine to yield the mono amide derivative which was hydrogenolysed to give the acid (CI-MS: m/z 265 [M+b]+).
出典と根拠
- ORDレコード
- ord-65c05d3a7c4048fa95c6e4a60246683b
- 出典データセット
- uspto-grants-1995_05
- 特許番号
- US05411984
反応ノート
読み込み中…