Styrene-4-sulfonyl chloride → N-hydroxy-2-phenylsuccinimide p-styrenesulfonate
反応式
[OH:1][N:2]1[C:6](=[O:7])[CH2:5][CH:4]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:3]1=[O:14].[CH2:15]=[CH:16][C:17]1[CH:22]=[CH:21][C:20]([S:23](Cl)(=[O:25])=[O:24])=[CH:19][CH:18]=1>CC(C)=O>[OH:1][N:2]1[C:6](=[O:7])[CH2:5][CH:4]([C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)[C:3]1=[O:14].[CH2:15]=[CH:16][C:17]1[CH:22]=[CH:21][C:20]([S:23]([O-:25])(=[O:1])=[O:24])=[CH:19][CH:18]=1参加物
4
実験手順
50 ml of acetone was added to 3.8 g of N-hydroxy-2-phenylsuccinimide and 4.1 g of p-styrenesulfonyl chloride and then the same procedure as that of Preparation Example 1 was repeated to obtain 4.3 g of N-hydroxy-2-phenylsuccinimide-p-styrenesulfonate.