1-Naphthalenesulfonyl chloride → N-hydroxymaleimide 1-naphthalenesulfonate
反応式
[OH:1][N:2]1[C:6](=[O:7])[CH:5]=[CH:4][C:3]1=[O:8].[C:9]1([S:19](Cl)(=[O:21])=[O:20])[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH:12]=[CH:11][CH:10]=1>CC(C)=O>[OH:1][N:2]1[C:6](=[O:7])[CH:5]=[CH:4][C:3]1=[O:8].[C:9]1([S:19]([O-:21])(=[O:1])=[O:20])[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH:12]=[CH:11][CH:10]=1参加物
4
実験手順
120 ml of acetone was added to 5.7 g of N-hydroxymaleimide and 11.3 g of 1-naphthalenesulfonyl chloride and then the same procedure as that of Preparation Example 1 was repeated to obtain 10.9 g of N-hydroxymaleimide-1-naphthalenesulfonate.
後処理
- customthe same procedure as that of Preparation Example 1
出典と根拠
- ORDレコード
- ord-844a59761d704f9a89b1c9e27d930a9d
- 出典データセット
- uspto-grants-1991_03
- 特許番号
- US05002853
反応ノート
読み込み中…