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Thionyl Chloride → 3-methoxy-4-nitro-benzoyl Chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-Methoxy-4-nitrobenzoic acid | HCID 78764 | — |
| 溶媒 | 2,2,4-Trimethylpentane | HCID 10907 | — |
| 生成物 | 3-methoxy-4-nitro-benzoyl Chloride | HCID 11127655 | — |
反応手順
A stirred suspension of 1.0 g of 3-methoxy-4-nitrobenzoic acid and 1.40 ml of thionyl chloride is heated to reflux for 2 hours. The mixture is cooled to room temperature, 2 ml of iso-octane added and the mixture evaporated in vacuo to a solid residue. The residue is washed with iso-octane (2×2 ml), dried in vacuo to give 1.08 g of cream colored solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05733905 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-bb6cde0faedc4e19ba217101110ea105 |
| 出典メモ | uspto-grants-1998_03 |