Ammonia → HCID 178434093、化合物

HRID 361266ノート

反応式

HRID 361266 の反応式
Cl.Cl.[NH2:3][C:4]1[C:5]([CH3:16])=[N:6][N:7]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[C:8]=1[NH2:9].[NH3:17]>O.C(O)C>[NH2:9][C:8]1[N:7]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[N:6]=[C:5]([CH3:16])[C:4]=1[N:3]=[C:4]1[C:8](=[NH:7])[NH:9][N:17]=[C:5]1[CH3:16]

参加物

5

反応物 2

HCID 222AmmoniaHCID 122269664,5-Diamino-3-methyl-1-phenyl pyrazole dihydrochloride

生成物 1

HCID 178434093HCID 178434093、化合物

試薬・触媒・溶媒 2

HCID 702Ethanol溶媒HCID 962Water溶媒

実験手順

2.6 g 4,5-diamino-3-methyl-1-phenyl-1H-pyrazole dihydrochloride were dissolved in a mixture of 30 ml water and 30 ml ethanol. The pH of the resulting solution was then adjusted to 9 with concentrated ammonia. Subsequently the reaction mixture was stirred for 17 hours with a gasifying stirrer. The precipitated dye compounds was separated by filtration, washed with water and dried. The yield amounted to 1.2 g.

後処理

  1. customThe precipitated dye compounds was separated by filtration
  2. washwashed with water
  3. customdried

出典と根拠

ORDレコード
ord-fa450293b83c4901bf8ec82c51978f49
出典データセット
uspto-grants-1999_02
特許番号
US05865855

反応ノート

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