関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dimethylformamide | HCID 6228 | — |
| 反応物 | 3-Chloro-2-methyl-1-propene | HCID 11241 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | N-Butylaniline | HCID 14310 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N-butyl-N-(2-methylprop-2-eneyl)aniline | HCID 54010992 | — |
反応手順
A mixture of N-butylaniline (12.35 parts), anhydrous potassium carbonate (17.1 parts), 3-chloro-2-methylpropene (11.24 parts) and DMF (20 parts) was stirred at 90° C. for 8 hours. The cooled mixture was poured into toluene, washed with water (×2), 1N hydrochloric acid (30 parts) and water (×2). The dried organic phase was evaporated to leave N-butyl-N-(2-methylprop-2-eneyl)aniline (14.3 parts).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05865857 |
|---|
| 出典データセット | uspto-grants-1999_02 |
|---|
| ORD ID | ord-6202f9c73b3f43119b22e8e6eec14055 |
|---|
| 出典メモ | uspto-grants-1999_02 |
|---|
