Imidazole → Imidazole isocyanuric acid

HRID 362598

反応式

HRID 362598 の反応式
[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[NH:6]1[C:13](=[O:14])[NH:12][C:10](=[O:11])[NH:9][C:7]1=[O:8]>>[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[NH:6]1[C:13](=[O:14])[NH:12][C:10](=[O:11])[NH:9][C:7]1=[O:8]

参加物

3

反応物 2

HCID 795ImidazoleHCID 7956Cyanuric acid

生成物 1

HCID 68522078Imidazole isocyanuric acid

実験手順

Heretofore, in a process for obtaining an adduct of imidazole-isocyanuric acid, water, aqueous solution of acetic acid, or dimethylformamide is used as a solvent. An imidazole compound and isocyanuric acid are charged into the solvent as it is in a solid to react by addition, and then crystallized while cooling, thereby being obtained an adduct of imidazole-isocyanuric acid. (confer JP-A-53-116391).

後処理

  1. customto react by addition
  2. customcrystallized
  3. temperaturewhile cooling

出典と根拠

ORDレコード
ord-523eaac753074f7b8ebf4e8ee6e19117
出典データセット
uspto-grants-1999_02
特許番号
US05869664

関連ノート

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