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HRID 363038作成日:2026年10月27日

Methyl 3-allyl-4-hydroxybenzoate → Methyl 4-hydroxy-3-propylbenzoate

https://huagongshe.com/reaction/363038

反応式

関与物質

役割名称HCID仕込み量
反応物Methyl 3-allyl-4-hydroxybenzoateHCID 939882—
触媒PalladiumHCID 23938—
溶媒Ethyl AcetateHCID 8857—
生成物Methyl 4-hydroxy-3-propylbenzoateHCID 11805593—

反応手順

To 22-3 (6.0 g, 33.2 mmol) in 50 mL of EtOAc was added 60 mg of 5% Pd on carbon and the whole was hydrogenated at atmospheric pressure for 24 h. Hydrogen was removed from the reaction mixture and the solution was filtered through Celite. Evaporation of the solvent afforded product 22-4 as a white solid.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05872138
出典データセットuspto-grants-1999_02
ORD IDord-f01451e0f3f640d8932c8f76d798ecf0
出典メモuspto-grants-1999_02