化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Dithionite → 1,3-Di-cyclopropyl-8-amino Xanthine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Dithionite | HCID 24489 | — |
| 反応物 | 1,3-Di-cyclopropyl-8-nitro xanthine | HCID 9838492 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 1,3-Di-cyclopropyl-8-amino Xanthine | HCID 9813621 | — |
反応手順
1,3-Di-cyclopropyl-8-nitro xanthine (0.4 g, 0.0014 mol) was dissolved in methanol (20 ml) and treated with a sodium dithionite solution in water (0.5 g in 5 ml) at room temperature with stirring. After stirring for three hours the solvent was removed in vacuo, the residue taken up with dichloromethane and extracted with water (40 ml).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05734051 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-6437b784cf604f0ba86ac0d067c33742 |
| 出典メモ | uspto-grants-1998_03 |