関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Anthranilic Acid | HCID 227 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | n-Octyl p-Toluenesulfonate | HCID 599296 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N-n-octylanthranilic acid | HCID 15090289 | 43.1% |
反応手順
To a solution of anthranilic acid in toluene, n-octyl p-toluenesulfonate prepared according to the conventional method was added and the mixture was refluxed at 120° C. After 6 hours, an aqueous solution of sodium hydroxide was added and the toluene layer was concentrated. N-n-octylanthranilic acid was obtained from the remaining reactant after the purification by column chromatography with the yield of 43.1%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05413794 |
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| 出典データセット | uspto-grants-1995_05 |
|---|
| ORD ID | ord-83f0afa4f03c4cc1a583fc651ef4429b |
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| 出典メモ | uspto-grants-1995_05 |
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