化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → ethyl N-n-octanoylanthranilate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 2-(Octanoylamino)benzoic acid | HCID 4157220 | — |
| 生成物 | ethyl N-n-octanoylanthranilate | HCID 4179835 | 89.2% |
反応手順
Thionyl chloride was dropped to ethanol and the mixture was stirred for 2 hours. Then, N-n-octanoylanthranilic acid was added to the mixture and reaction was allowed to proceed for 3 days at the room temperature. After the reaction, the solvent was removed and ethyl N-n-octanoylanthranilate was obtained from the remaining reactant after the purification by column chromatography with the yield of 89.2 %.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05413794 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-6973f46854414d4d8229c43ebb702f0c |
| 出典メモ | uspto-grants-1995_05 |