関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | N-Methylbutylamine | HCID 8068 | — |
| 反応物 | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| 生成物 | N-butyl-N-methylacetamide dimethyl acetal | HCID 19379602 | — |
反応手順
6.1 g (0.07 mol) of n-butylmethylamine are stirred with 9.3 g (0.07 mol) of N,N-dimethylacetamide dimethyl acetal for 24 hours under reflux at a bath temperature of 130° C. Subsequent vacuum distillation gives N-butyl-N-methylacetamide dimethyl acetal, bp 72°-75° C./31 mbar.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05413994 |
|---|
| 出典データセット | uspto-grants-1995_05 |
|---|
| ORD ID | ord-958d91a3e3b94844878d9825f3955bb5 |
|---|
| 出典メモ | uspto-grants-1995_05 |
|---|
